Table 5: Indexed X-ray diffraction data of [UO2(L1)(CH3OH)] complex.
| Peak no. | d (obs.) | d (cal.) | Int. wt. | 2θ (obs.) | 2θ (cal.) | SinSqTheta*E4 (obs.) | SinSqTheta*E4 (cal.) | h | k | l |
| 1 | 12.1158 | 12.0528 | 1.0 | 7.29 | 7.33 | 40.4 | 40.8 | 0 | 1 | 0 |
| 2 | 9.6357 | 9.5928 | 1.0 | 9.17 | 9.21 | 63.9 | 64.5 | 0 | 1 | 1 |
| 3 | 8.5809 | 8.5685 | 1.0 | 10.30 | 10.31 | 80.6 | 80.8 | 1 | 1 | 0 |
| 4 | 6.1245 | 6.1358 | 1.0 | 14.45 | 14.42 | 158.2 | 157.6 | 1 | 1 | 1 |
| 5 | 5.2883 | 5.3004 | 1.0 | 16.75 | 16.71 | 212.1 | 211.2 | 2 | 0 | 0 |
| 6 | 4.8177 | 4.8367 | 1.0 | 18.40 | 18.33 | 255.6 | 253.6 | 1 | 0 | 2 |
| 7 | 3.8064 | 3.8075 | 1.0 | 23.35 | 23.34 | 409.5 | 409.3 | 2 | 2 | 1 |
| 8 | 3.6836 | 3.6776 | 1.0 | 24.14 | 24.18 | 437.3 | 438.7 | 3 | 0 | 1 |
| 9 | 3.3249 | 3.3230 | 1.0 | 26.79 | 26.81 | 536.7 | 537.3 | 3 | 0 | 2 |
| 10 | 3.0223 | 3.0199 | 1.0 | 29.53 | 29.55 | 649.5 | 650.5 | 2 | 2 | 1 |
| 11 | 2.9274 | 2.9264 | 1.0 | 30.51 | 30.52 | 692.3 | 692.8 | 1 | 3 | 1 |
| 12 | 2.5693 | 2.5680 | 1.0 | 34.89 | 34.91 | 898.7 | 899.7 | 1 | 5 | 2 |
| 13 | 2.4018 | 2.4014 | 1.0 | 37.41 | 37.42 | 1028.5 | 1028.8 | 3 | 2 | 4 |
| 14 | 2.2365 | 2.2357 | 1.0 | 40.29 | 40.31 | 1186.1 | 1187.0 | 4 | 1 | 1 |
| 15 | 2.1416 | 2.1413 | 1.0 | 42.16 | 42.17 | 1293.6 | 1293.9 | 4 | 1 | 2 |
| 16 | 2.1007 | 2.1003 | 1.0 | 43.02 | 43.03 | 1344.4 | 1344.9 | 4 | 4 | 2 |
| 17 | 1.9481 | 1.9470 | 1.0 | 46.58 | 46.61 | 1563.3 | 1565.0 | 3 | 5 | 3 |
| 18 | 1.9091 | 1.9080 | 1.0 | 47.59 | 47.62 | 1627.8 | 1629.7 | 3 | 4 | 1 |
| 19 | 1.8889 | 1.8872 | 1.0 | 48.13 | 48.18 | 1662.8 | 1665.8 | 3 | 6 | 2 |
| 20 | 1.8202 | 1.8202 | 1.0 | 50.07 | 50.07 | 1790.7 | 1790.8 | 5 | 4 | 3 |
| Unit cell data and crystal lattice parameters | ||||||||||
| a = 11.0800 Å | V = 1377.79 Å3 | |||||||||
| b = 13.2700 Å | ||||||||||
| c = 10.6800 Å | Crystal system: triclinic | |||||||||
| α = 113.500° D | Nature: crystalline | |||||||||
| β = 104.980° | Particle size = 44 nm | |||||||||
| γ = 91.105° | ||||||||||